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高溫高壓光學(xué)浮區(qū)爐

SciDre單晶爐特點(diǎn)

● 采用垂直式光路設(shè)計(jì)

● 采用高照度短弧氙燈，多種功率規(guī)格可選

● 熔區(qū)溫度：>3000℃

● 熔區(qū)壓力：10bar/50bar/100bar/150bar/300bar等多種規(guī)格可選

● 氧氣/氬氣/氮?dú)?空氣/混合氣等多種氣路可選

● 采用光柵控制技術(shù)，加熱功率從0-100% 連續(xù)可調(diào)

● 樣品腔可實(shí)現(xiàn)低至10-5mbar真空環(huán)境

● 豐富的可升級(jí)選件

SciDre單晶爐技術(shù)參數(shù)

熔區(qū)溫度：高達(dá)2000 - 3000℃以上

熔區(qū)壓力：高至10、50、100、150、300 bar可選

熔區(qū)真空：1*10-2 mbar或 1*10-5 mbar可選

熔區(qū)氣氛：Ar、O2、N2等可選

氣體流量：0.25 – 1 L/min流量可控

氙燈功率：3kW至15kW可選

料棒臺(tái)尺寸：6.8mm或9.8mm可選

拉伸速率：0.1-50mm/h

調(diào)節(jié)速率：0.6 mm/s

拉伸尺寸：130mm，150mm，195mm可選

旋轉(zhuǎn)速率：0-70rpm

用電功率：400V三相 63A 50Hz

主機(jī)尺寸：330cm*163cm*92cm （不同規(guī)格略有差異）

發(fā)表文章

1. (2020)Single crystal growth and luminescent properties of YSH:Eu scintillator by optical floating zone method Chemical Physics Letters， Volume 738， 136916

2. (2020)Anisotropic character of the metal-to-metal transition in Pr4Ni3O10 Phys. Rev. B 101， 104104

3. (2020)Synthesis of a New Ruthenate Ba26Ru12O57 Crystals 2020， 10(5)， 355

4. (2020)Synthesis and characterization of bulk Nd1- SrxNiO2 and Nd1- xSrxNiO3 Phys. Rev. Materials 4， 084409

5. (2020)Magnetic phase diagram and magnetoelastic coupling of NiTiO3 Phys. Rev. B 101， 195122

6. (2019)High pO2 Floating Zone Crystal Growth of the Perovskite Nickelate PrNiO3 Crystals 2019， 9(7)， 324

7. (2019)Magnetic properties of high-pressure optical floating-zone grown LaNiO3 single crystals Journal of Crystal Growth Volume 524， 15 October 2019， 125157

8. (2019)Bulk single-crystal growth of the theoretically predicted magnetic Weyl semimetals RAlGe (R = Pr， Ce) Phys. Rev. Materials 3， 024204

9. (2019)Pushing boundaries: High pressure， supercritical optical floating zone materials discovery Journal of Solid State Chemistry 270 (2019): 705-709

10. (2018). Antiferromagnetic correlations in the metallic strongly correlated transition metal oxide LaNiO3. Nature Communications 9:43

11. (2017). Single-crystal growth and physical properties of 50% electron-doped rhodate Sr 1.5 La 0.5 RhO 4 Physical Review Materials 1(4)， 044005

12. (2017). Single crystal growth and structural evolution across the 1st order valence transition in (Pr1-yYy) 1- xCaxCoO3-δJournal of Solid State Chemistry 254， 69-74

13. (2017). Large orbital polarization in a metallic square-planar nickelate. Nature Physics 13， 864–869

14. (2017). High-Pressure Floating-Zone Growth of Perovskite Nickelate LaNiO3 Single Crystals. Crystal Growth & Design 17(5)， 2730-2735.

15. (2017). High-pressure optical floating-zone growth of Li(Mn，F(xiàn)e)PO4 single crystals. Journal of Crystal Growth， 462， 50-59.

16. (2016). Evidence for a spinon Fermi surface in a triangular-lattice quantum-spin-liquid candidate. Nature 540， 559–562.

17. (2016). Stacked charge stripes in quasi-2D trilayer nickelate La4Ni3O8. PNAS 2016 113 (32) 8945-8950.

18. (2016). Single Crystal Growth of Pure Co3+ Oxidation State Material LaSrCoO4. Crystals， 6(8)， 98.

19. (2015). Floating zone growth of Ba-substituted ruthenate Sr2?xBaxRuO4. Journal of Crystal Growth， 427， 94-98.

20. (2015). High pressure floating zone growth and structural properties of ferrimagnetic quantum paraelectric BaFe12O19. APL Materials 3， 062512.

21. (2015). Impact of local order and stoichiometry on the ultrafast magnetization dynamics of Heusler compounds. Journal of Physics D: Applied Physics， 48(16)， 164016.

22. (2014). Brownmillerite Ca2Co2O5: Synthesis， Stability， and Re-entrant Single Crystal to Single Crystal Structural Transitions. Chemistry of Materials， 26(24)， 7172-7182.

23. (2014). Low-temperature properties of single-crystal CrB2. Physical Review B， 90(6)， 064414.(Also on archiv.org.)

24. (2014). Effect of annealing on spinodally decomposed Co2CrAl grown via floating zone technique. Journal of Crystal Growth， 401， 617-621.(Also on arxiv.org.)

25. (2013). de Haas–van Alphen effect and Fermi surface properties of single-crystal CrB2. Physical Review B， 88(15)， 155138. (Also on arxiv.org.)

26. (2013). Phase Dynamics and Growth of Co2Cr1–xFexAl Heusler Compounds: A Key to Understand Their Anomalous Physical Properties. Crystal Growth & Design， 13(9)， 3925-3934.

27. (2011). Exploring the details of the martensite–austenite phase transition of the shape memory Heusler compound Mn2NiGa by hard x-ray photoelectron spectroscopy， magnetic and transport measurements. Applied Physics Letters， 98(25)， 252501.

28. (2011). Challenges in the crystal growth of Li2CuO2 and LiMnPO4. Journal of Crystal Growth， 318(1)， 995-999.

29. (2011). Self-flux growth of large EuCu 2 Si 2 single crystals. Journal of Crystal Growth， 318(1)， 1043-1047.

30. (2010). Influence of heat distribution and zone shape in the floating zone growt·h of selected oxide compounds. Journal of materials science， 45(8)， 2223-2227.

31. (2009). Highly ordered， half-metallic Co2FeSi single crystals. Applied Physics Letters， 95(16)， 161903.

32. (2009). Single-crystal growth of LiMnPO4 by the floating-zone method. Journal of Crystal Growth， 311(5)， 1273-1277(Also on uni-heidelberg.de.)

33. (2008). Crystal growth of rare earth-transition metal borocarbides and silicides. Journal of Crystal Growth， 310(7)， 2268-2276.

用戶單位

中國科學(xué)院物理研究所

中國科學(xué)院固體物理研究所

北京師范大學(xué)

中山大學(xué)

南昌大學(xué)

上海大學(xué)